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The level of Cys18 peptide oxidation was calculated as the percentage of the peak area of the oxidized Cys18 peptide (alkylated with 13 C 2 ,D 2 - ioodacetamide ) over the sum of the reduced Cys18 peptide (alkylated with 13 C 0 ,D 0 - iodoacetamide ) and oxidized Cys18 peptide as shown below: Other biochemical measurements Plasma GPx activity was measured as detailed previously 10

AA holds a Sara Borrell research contract (CD17/0146) supported by ISCIII from MINECO [confounded by the European Social Fund (ESF)]

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Transient headache and mild facial flushing have been noted in some protocols

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